期刊论文

Wujiu Jiang<&wdkj&>Yuxing Tan

英文

Journal of Inorganic Biochemistry

0162-0134

2022

232

111808

10.1016/j.jinorgbio.2022.111808

CRediT authorship contribution statement Wujiu Jiang: Conceptualization, Methodology, Writing – original draft, Writing – review & editing. Qiqi Qin: Investigation, Validation, Formal analysis. Xiyuan Xiao: Validation, acquisition. Yuxing Tan: Project administration, Writing – original draft, Writing – review & editing, acquisition.

本校为第一机构

Eight new diorganotin(IV) complexes (1a-2d), namely {[X-C6H4(O)C=N-N=C(Me)COO]R2Sn(CH3OH)}(n) (1a, 2a), {[X-C6H4(O)C=N-N=C(Me)COO]R2Sn(CH3OH)}(2) (1b, 1c, 1d, 2b), and {[X-C6H4(O)C=N-N=C(Me)COO]R2Sn}(2) (2c, 2d) (X = H-, p-Me-, p-OH-, p-NO2-; R = o-Cl-C6H4CH2- or o-Me-C6H4CH2-), have been synthesized by microwave "one-pot" reaction with arylformylhydrazine, pyruvic acid, and the corresponding R2SnCl2. All the complexes have been characterized by FT-IR (Fourier transform infrared spectroscopy), multinuclear NMR (H-1, C-13, and Sn-119 nuclear magnetic resonance spectroscopies), HRMS (high-resolu...