邻氟苄基氯和间氟苄基氯在适当的溶剂中与锡粉反应,合成了二(邻氟苄基)二氯化锡(1)和二(间氟苄基)二氯化锡(2),经 X射线衍射方法测定了新化合物的晶体结构。化合物1属单斜晶系,空间群为C2/c,晶体学参数:a =2.3663(7)nm,b =0.48358(14)nm,c =1.2699(4)nm,β=93.789(4)°,V =1.4500(8) nm3,Z=4,Dc=1.868 g/cm3,μ(Mo Kα)=21.35 cm-1,F(000)=792,R1=0.0423,Rw =0.1174。化合物2属单斜晶系,空间群为C2/c,晶体学参数:a =2.3824(3)nm,b =0.47915(5)nm,c =1.28157(14)nm,β=94.142(2)°,V =1.4591(3)nm3,Z =4,Dc =1.856 g/cm3,μ(MoKα)=2.121 cm-1, F(000)=792,R1=0.0213,wR2=0.0458;中心锡原子为...