The fabrication of poly (polyethylene glycol diacrylate) monolithic porous layer open tubular (mono-PLOT) columns and applications in hydrophilic interaction chromatography and capillary gas chromatography for small molecules

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作者信息关键词期刊信息基础信息归属信息摘要

成果类型：

期刊论文

作者：

Chang, Feng;Yue, Yunfang;Yang, Zihui;Huang, Si;Liu, Zhihua;...

通讯作者：

Chen, Yingzhuang

作者机构：

[Yang, Zihui; Yue, Yunfang; Chen, Yingzhuang; Chang, Feng; Huang, Si; Chen, Bo; Ma, Ming] Hunan Normal Univ, Key Lab Phytochem R&D Hunan Prov, Key Lab Chem Biol & Tradit Chinese Med Res, Minist Educ, Changsha, Hunan, Peoples R China.

[Liu, Zhihua; Wang, Kunmiao] China Tobacco Yunnan Ind Co Ltd, Key Lab Tobacco Chem Yunnan Prov, Res & Dev Ctr, Kunming, Yunnan, Peoples R China.

[Peng, Yan] Hengyang Normal Univ, Coll Econ & Management, Hengyang, Peoples R China.

通讯机构：

[Chen, Yingzhuang] H

Hunan Normal Univ, Key Lab Phytochem R&D Hunan Prov, Key Lab Chem Biol & Tradit Chinese Med Res, Minist Educ, Changsha, Hunan, Peoples R China.

语种：

英文

关键词：

Aqueous two-phase polymerization;Capillary liquid chromatography;Gas chromatography;Hydrophilic chromatography;Porous layer open tubular

期刊：

ELECTROPHORESIS

ISSN：

0173-0835

年：

2019

卷：

期：

页码：

521-529

DOI：

10.1002/elps.201800410

基金类别：

Natural Science Foundation of Hunan ProvinceNatural Science Foundation of Hunan Province [2018JJ2251]; National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21305040, 21775040]

机构署名：

本校为其他机构

院系归属：

经济与管理学院

摘要：

The easy shrinkage and swelling of polymer monolithic column when exposed to mobile phase with different polarity is a problem that cannot be ignored. To overcome this drawback, a convenient aqueous two-phase polymerization approach was used to prepare poly (polyethylene glycol diacrylate, PEGDA) monolithic porous layer open tubular (mono-PLOT) columns (150 μm). The poly(PEGDA) mono-PLOT column with homogeneous polymer porous layer was synthesized successfully. A maximum plate number of 41,500 plates per meter for allyl thiourea was obtained u...

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The fabrication of poly (polyethylene glycol diacrylate) monolithic porous layer open tubular (mono-PLOT) columns and applications in hydrophilic interaction chromatography and capillary gas chromatography for small molecules

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