A catalyst-free and additive-free method for the synthesis of benzothiazolethiones from o-iodoanilines, DMSO and potassium sulfide

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成果类型：

期刊论文

作者：

Zhu, Xiaoming;Li, Wenguang;Luo, Xiai;Deng, Guobo;Liang, Yun*;...

通讯作者：

Liang, Yun;Liu, Jianbing

作者机构：

[Liu, Jianbing; Liang, Yun; Liu, JB; Zhu, Xiaoming; Deng, Guobo; Li, Wenguang; Luo, Xiai] Hunan Normal Univ, Key Lab Chem Biol & Tradit Chinese Med Res, Natl & Local Joint Engn Lab New Petrochem Mat & F, Minist Educ,Key Lab Assembly & Applicat Organ Fun, Changsha 410081, Hunan, Peoples R China.

[Zhu, Xiaoming] Hengyang Normal Univ, Key Lab Funct Met Organ Cpds Hunan Prov, Coll Chem & Mat Sci, Hunan Prov Univ Key Lab Funct Organometall Mat, Hengyang 421008, Hunan, Peoples R China.

通讯机构：

[Liang, Y; Liu, JB] H

Hunan Normal Univ, Key Lab Chem Biol & Tradit Chinese Med Res, Natl & Local Joint Engn Lab New Petrochem Mat & F, Minist Educ,Key Lab Assembly & Applicat Organ Fun, Changsha 410081, Hunan, Peoples R China.

语种：

英文

期刊：

Green Chemistry

ISSN：

1463-9262

年：

2018

卷：

期：

页码：

1970-1974

DOI：

10.1039/c8gc00477c

基金类别：

National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21572051, 21602057]; Ministry of Education of the People's Republic of ChinaMinistry of Education, China [213027A]; Education Department of Hunan Province [15A109]; Aid Programs for Technology Innovative Team and Key Discipline in Education Department of Hunan Province; Opening Fund of Key Laboratory of Chemical Biology and Traditional Chinese Medicine Research (Ministry of Education of China)Ministry of Education, China; Hunan Normal University [KLCBTCMR201707, KLCBTCMR201708]

机构署名：

本校为其他机构

院系归属：

化学与材料科学学院

摘要：

Under catalyst-free and additive-free conditions, a novel, convenient, eco-friendly method for the synthesis of benzothiazolethiones has been developed. The three-component reaction of o-iodoanilines and K2S with DMSO proceeded smoothly and the corresponding benzothiazolethiones were obtained with good isolated yields. Meanwhile, this method could be used for the synthesis of thioureas from primary diamines. Furthermore, mechanism research showed that DMSO not only functioned as a...

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A catalyst-free and additive-free method for the synthesis of benzothiazolethiones from o-iodoanilines, DMSO and potassium sulfide

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