版权说明 操作指南
首页 > 成果 > 详情

Synthesis and Crystal Structure of a Hexameric Organooxotin Cluster from Benzilic Acid

认领
导出
反馈
分享
QQ微信 微博
成果类型:
期刊论文
作者:
Chen, MS;Kuang, DZ*;Zhang, CH;Deng, YF;Li, W;...
通讯作者:
Kuang, DZ
作者机构:
[Deng, YF; Yang, YQ; Li, W; Chen, MS; Kuang, DZ; Zhang, CH] Hengyang Normal Univ, Dept Chem & Mat Sci, Hengyang 421008, Peoples R China.
通讯机构:
[Kuang, DZ] H
Hengyang Normal Univ, Dept Chem & Mat Sci, Hengyang 421008, Peoples R China.
语种:
英文
关键词:
organooxotin cluster;benzilic acid;crystal structure;synthesis organooxotin cluster;benzilic acid;crystal structure;synthesis
关键词(中文):
二苯乙醇酸;合成方法;晶体结构;有机锡
期刊:
Chinese Journal of Structural Chemistry
ISSN:
0254-5861
年:
2005
卷:
24
期:
11
页码:
1249-1253
基金类别:
This work was ;supported by the Natural Science Foundation of Hunan Province;and Project supported by Science Foundation of Hengyang Normal University of China
机构署名:
本校为第一且通讯机构
院系归属:
化学与材料科学学院
摘要:
The title complex [^n BuSn(O)O2C(OH)CPh2]6.2H2O has been synthesized by the reaction of n-BuSn(O)OH with benzilic acid in 1:1 molar radio and characterized by IR, ^1H NMR spectra and elemental analysis. The crystal structure was determined by X-ray diffraction. It crystallizes in triclinic, space group PI with a = 1.3543(2), b = 1.4593(2), c = 1.5293(2) nm, α = 102.075 (2),β = 115.571 (2), γ = 93.308(3)°, Z = 1, V = 2.6282(7) nm^3, Mr = 2550.21, Dc = 1.611 g/cm^3,μ = 1.477 mm^-1, F(000) = 1280, R = 0.0309 and wR = 0....

反馈

验证码:
看不清楚,换一个
确定
取消

成果认领

标题:
用户 作者 通讯作者
请选择
请选择
确定
取消

提示

该栏目需要登录且有访问权限才可以访问

如果您有访问权限,请直接 登录访问

如果您没有访问权限,请联系管理员申请开通

管理员联系邮箱:yun@hnwdkj.com