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Synthesis, Crystal Structure and Electrochemical Properties of [Ni(phen)_3]·(m-nitrobenzoic acid)_2·(H_2O)

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成果类型:
期刊论文
作者:
Kuang Yun-Fei;Li Chang-Hong;Li Wei;Yang Ying-Qun
通讯作者:
Kuang, YF
作者机构:
[Kuang Yun-Fei; Li Wei; Yang Ying-Qun] Department of Chemistry and Materials Science, Hengyang Normal University
[Li Chang-Hong] Department of Chemistry and Chemical Engineering, Hunan Institute of Technology
通讯机构:
[Kuang, YF ]
Hengyang Normal Univ, Dept Chem & Mat Sci, Hengyang 421008, Peoples R China.
语种:
英文
关键词:
nickel(II) complex;crystal structure;electrochemical property
关键词(中文):
镍(Ⅱ);配合物;晶体结构;电气化学性质;合成
期刊:
Chinese Journal of Structural Chemistry
ISSN:
0254-5861
年:
2007
卷:
26
期:
7
页码:
749-752
基金类别:
Supported by the Foundation of Education Committee of Hunan Province (06C 195) and the Research Award Fund for 0utstanding Young Teachers of Hengyang Normal University (2006)
机构署名:
本校为第一且通讯机构
院系归属:
化学与材料科学学院
摘要:
A new nickel(II) coordination complex [Ni(phen)3]·(m- nitrobenzoic acid)2-(H2O) was synthesized by self-assembly of m-nitrobenzoic acid, 1,10-phenanthroline and nickelous Perchlorate. It crystallizes in the monoclinic system, space group C2/c, with a = 2.4596(6), b = 1.2124(3), c = 1.9824(5) nm, β = 97.088(5)°, V = 5.866(3) nm 3, Dc = 1.474 g/cm3, Z = 4, Mr = 1301.82, μ(MoKα) = 0.417 mm-1 F(000) = 2688, R - 0.0493 and wR = 0.1025. Structural determination indicates that the nickel(II) ion is coordinated with six nitrogen atoms from three p...

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