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Synthesis,Crystal Structure and Electrochemical Properties of a Cadmium(Ⅱ) Complex with α-Furoic Acid and 1,10-Phenanthroline

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成果类型:
期刊论文
作者:
Zhang Shao-Hua*;Li Chang-Hong;Li Wei;Yang Ying-Qun
通讯作者:
Zhang Shao-Hua
作者机构:
[Yang Ying-Qun; Zhang Shao-Hua; Li Wei] Hengyang Normal Univ, Dept Chem & Mat Sci, Hengyang 421008, Peoples R China.
[Li Chang-Hong] Hunan Inst Technol, Dept Chem Engn, Hengyang 421002, Peoples R China.
通讯机构:
[Zhang Shao-Hua] H
Hengyang Normal Univ, Dept Chem & Mat Sci, Hengyang 421008, Peoples R China.
语种:
英文
关键词:
cadmium(II) complex;crystal structure;electrochemical property analysis
关键词(中文):
镉(Ⅱ);络合物;晶体结构;电气化学
期刊:
Chinese Journal of Structural Chemistry
ISSN:
0254-5861
年:
2008
卷:
27
期:
10
页码:
1261-1264
基金类别:
Supported by the construct program of the key discipline in hunan province. and the Research Award Fund for the Outstanding Young Teachers of Hengyang Normal University (2006)
机构署名:
本校为第一且通讯机构
院系归属:
化学与材料科学学院
摘要:
A new cadmium complex [Cd(phen)3]-(ClO4) 2-(α-FRA)(H2O)3 was prepared by self-assembly of α-furoic acid, 1,10-phenanthroline (phen), and cadmium perchlorate. It crystallizes in the monoclinic system, space group P2 1/n, with a = 1.28130(15), b = 2.5957(3), c = 1.35449(16) nm, β = 109.395(2)°, V = 4.2492(9) nm3 Dn = 1.491 g/cm 3, Z = 4, F(000) = 1926, GOOF = 1.023, the final R = 0.0729 and wR - 0.2086. The crystal structure analysis indicates that the cadmium ion is coordinated with six nitrogen atoms from six 1, 10-phenanthroline molecules,...

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