期刊论文

Kuang Dai-Zhi

英文

Chinese Journal of Structural Chemistry

0254-5861

2008

27

12

1514-1518

Supported by the Key Foundation of Educational Department of Hunan Province （06A009）, the Construct Program of the Key Discipline in Hunan Province, the Science and Technology Projcet of Hunan Province （2008FJ3026）, and Hengyang Bureau of Science ＆ Technology （06kj 17）

本校为第一且通讯机构

The title compound was prepared by the reaction of di(2,4,6-trichlorobenzyl) stannic chloride with quinoline-2-formate and characterized with elemental analysis, 1H NMR, IR and X-ray diffraction methods. It crystallizes in monoclinic, space group P2_1/n with a = 1.3138(3), b = 1.8756(4), c = 1.4599(3) nm, β = 92.731(3)°, V = 3.5933(12) nm~3, Z = 4, D_c = 1.795 g/cm~3, μ(MoKα) = 1.425 mm~(-1), F(000) = 1920, R = 0.0778, w_R = 0.2286 (for I > 2σ(I)) and R = 0.0932, w_R = 0.2415 (for all data). The independent reflections were 6359, among whi...