期刊论文

Zhang Fu-Xing

英文

Chinese Journal of Structural Chemistry

0254-5861

2010

29

10

1529-1535

10.14102/j.cnki.0254-5861.2010.10.012

Project supported by the Key Foundation of Education Committee of Hunan Province （10A014、10K010）； Key Subject Foundation of Hunan Province and SRTP Foundation of Hunan Province；

本校为第一且通讯机构

The dibutyltin 3,4-dimethoxybenzotate compound {[（3,4-（CH3O）2C6H3COO） Sn（Bu-n）2]2O}2 has been synthesized by the reaction of dibutyltin oxide with 3,4-dimethoxybenzoic acid. Its structure was determined by X-ray single-crystal diffraction. The crystal belongs to the triclinic system,space group P1 with a = 1.2003（2）,b = 1.2821（3）,c = 1.3666（3） nm,α = 80.50（3）,β = 65.56（3）,γ = 73.36（3）°,Z = 2,V = 1.8318（6） nm3,Dc = 1.530 Mg·m-3,μ（MoKa） = 1.413 mm-1,F（000） = 860,R = 0.0554 and wR = 0.1092. In the complex,each tin ato...