期刊论文

Kuang Dai-Zhi

英文

Chinese Journal of Structural Chemistry

0254-5861

2012

31

9

1241-1246

10.14102/j.cnki.0254-5861.2012.09.003

Sponsored by the Natural Science Foundation of Hunan Province （No. 11J J302 I）, the Innovation Platform Open fund of Hunan Provincial Education Department （No.09K099 and No. 10K010） and a key project （No. 10A014）, the Hunan Provincial Scientific Program （No.2010JT4041）, the open fund of the Key Laboratory of Functional Organometallic Materials of Colleges of Hunan Province （No. 10K02）, Hengyang Municipal Scientific Program （2011KG56）, and the Youth Program of Hengyang Normal University （No. 11 A28）

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The tris[（2-methyl-2-phenyl）propyl]（2,4-dinitro-phenolato）tin was synthesized by the reaction of bis[tri（2-methyl-2-phenyl）propyltin] oxide with 2,4-dinitrophenol. The compound was characterized by IR, 1H NMR spectra and elemental analysis. The crystal structure has been determined by X-ray diffraction. The crystal belongs to the monoclinic system, space group P21/n with a = 0.9649（0）, b = 1.0087（8）, c = 3.4867（4） nm, β = 90.965（7） , Z = 4, V = 3.3933（7） nm3, Dc = 1.369 Mg·m-3, （MoKa） = 0.796 mm-1, F（000） = 1440, R = 0.034...