期刊论文

Kuang Dai-Zhi

英文

Chinese Journal of Structural Chemistry

0254-5861

2014

33

10

1521-1526

10.14102/j.cnki.0254-5861.2014.10.039

Supported by Natural Science Foundation of Hunan Province（No.13JJ3112） Scientific ＆ Technological Projects of Hunan Province（No.2013TZ2025,2014NK3086） Open Foundation of Innovation Platform of Hunan Provincial University（No.13K105,14K014） Scientific ＆ Technological Projects of Hengyang City（No.2012KJ30） Cultivation projects Based on Collaborative Innovation Center of Hengyang Normal University（No.12XT02） the Youth Backbone Teacher Training Program of Hengyang Normal University（2012）

本校为第一且通讯机构

Two dinuclear organotin complexes C_8H_(14)(CO_2SnCy_3)_2 (1) (Cy = cyclohexyl group) and C_8H_(14)[CO_2Sn(CH_2CMe_2Ph)_3]_2 (2) were synthesized by the reactions of camphoric acid with tricyclohexyltin hydroxide and bis[tri(2-methyl-2-phenyl)propyltin] oxide under solvothermal conditions, and these complexes were characterized by infrared spectra, elemental analyses, and H NMR spectra. The crystal of 1 belongs to the monoclinic system, space group P2_1/c with a = 1.83478(19), b = 1.52707(18), c = 1.9849(2) nm,β= 122.515(7)°, Z= 4, V= 4.6896(...