期刊论文

Kuang Dai-Zhi

英文

Chinese Journal of Structural Chemistry

0254-5861

2015

34

11

1652-1658

10.14102/j.cnki.0254-5861.2011-0779

Natural Science Foundation of Hunan ProvinceNatural Science Foundation of Hunan Province [13JJ3112]; Scientific & Technological Projects of Hunan Province [2013TZ2025, 2014NK3086, 2014FJ3060]; Open Fund Project of Key Laboratory of Functional Organometallic Materials of Hengyang Normal University [13K105, 14K014, 13K01-05, GN14K01]; Aid Programs for Science and Technology Innovative Research Team in Higher Educational Institutions of Hunan Province; Key Discipline of Hunan Province; Scientific Research Fund of Hunan Provincial Education Department of ChinaHunan Provincial Education Department [15C0199, 15C0200, 14C0171, 14C0168]; Science Foundation of Hengyang Normal University of China [12C45]

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Bis(tricyclohexyltin) pimelicarboxylate, [(CH_2)_5(CO_2SnCy_3)_2] (1), has been synthesized by the reaction of tricyclohexyltin hydroxide with pimelic acid and characterized by means of IR, ~1H and ~(13)C NMR, elemental analysis and X-ray diffraction. Complex 1 crystallizes in triclinic space group P-bar1 with a = 11.569(3), b = 12.0419(2), c = 17.3988(4) A, a = 81.4310(10), β= 79.8270(10), γ = 69.7060(10)°, V = 2227.60(9) A~3, Z = 2, C_43H_(76)O_4Sn_2, M_r = 894.42, D_c = 1.333 g?cm~(-3), μ = 1.157 mm~(-1), F(000) = 932, GOOF = 1.339, the ...