期刊论文

Zhang Fu-Xing

英文

Chinese Journal of Structural Chemistry

0254-5861

2016

35

10

1510-1516

10.14102/j.cnki.0254-5861.2011-1194

Open Fund Project of Key Laboratory of Functional Organometallic Materials of Hengyang Normal University [15K017, 14K014, 13K105]; Natural Science Foundation of Hunan ProvinceNatural Science Foundation of Hunan Province [13JJ3112]; Scientific & Technological Projects of Hunan Province [2014NK3086]; Aid programs for Science and Technology Innovative Research Team in Higher Educational Institutions of Hunan Province; Key Discipline of Hunan Province; Project funding for research and innovation experiment of university students in Hunan Province; Scientific Research Fund of Hunan Provincial Education Department of ChinaHunan Provincial Education Department [14C0171, 14C0168, 15C0199, 15C0200]

本校为第一且通讯机构

μ_2-O-and μ_2-dimethylglyoximato-bridged μ_3-O-tris[di(m-fluorobenzyl)tin] bis(dimethylglyoximate) (1) has been synthesized by the reaction of di(m-fluorobenzyl)tin dichloride with dimethylglyoxime. Complex 1 was characterized by means of IR, ~1H NMR, elemental analysis and X-ray diffraction. It crystallizes in orthorhombic system, space group Pna2_1 with a = 2.22172(12), b = 1.05566(6), c = 2.15577(12) nm, V = 5.0561(5) nm~3, Z = 4, C_(50)H_(50)F_6N_4O_6Sn_3, M_r = 1273.01, D_c = 1.6721 g/cm~3, μ(MoΚα) = 15.44 cm~(-1), F(000) = 2520, R =...