期刊论文

Jiang Wu-Jiu;Tan Yu-Xing

英文

Chinese Journal of Structural Chemistry

0254-5861

2020

39

11

1965-1972

10.14102/j.cnki.0254-5861.2011-2747

(No,167 and 168):Supported by Hengyang Normal University College Students Scientific and Technological Works Project (No,GN19K07):Foundation of Key Laboratory of Functional Organometallic Materials,University of Hunan Province (No,19C0279):Scientific Research Fund of Hunan Provincial Education Department of China (Nos,HXKJ201908,HXKJ201911,HXKJ201946 and HXKJ201947):and Hengyang Normal University Industrial Supported Project

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Diorganotin 2-(2-(4-methoxybenzoyl)hydrazono)-3-phenylpropanoic carboxylate complexes I {[p-CH3O-C6H4O(O)C=N-N=C(PhCH2)COO](n-Bu)(2)Sn(CH3OH)}(2) and II [p-CH3O-C6H4O(O)C=N-N=C(PhCH2)COO](PhCH2)(2)Sn(CH3OH)}(2) have been synthesized. The complexes have been characterized by IR, H-1, C-13 and Sn-119 NMR spectra, FIRMS, elemental analysis, thermal stability analysis and the crystal structures have been determined by X-ray diffraction. The crystal of complex I belongs to triclinic system, space group P (1) over bar with a = 10.437(2), b = 11.576(3), c = 13.085(3) angstrom, alpha = 66.272(2)degree...