Cobalt phosphate materials were prepared in the present work in one step at room temperature using different raw materials and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS), and N2 gas adsorption. Cobalt phosphates exhibit 3D flower-like structures, and the assembly of nanosheets (petals of the “flowers”) of cobalt phosphate prepared with sodium phosphate and cobalt acetate as raw materials (denoted as Co-P(A)) is more incompact than that of cobalt phosphate prepared with ...
