Synthesis and crystal structure of 2-(4-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylic acid

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成果类型：

期刊论文

作者：

M. Zhang;G.-C. Ou;L. Yuan;G.-K. Jia;X.-Y. Yuan

通讯作者：

Yuan, X.-Y.

作者机构：

[Yuan X.-Y.; Zhang M.; Jia G.-K.] Department of Biology and Chemistry, Hunan University of Science and Engineering, Yongzhou, Hunan, China

Key Laboratory of Functional Organometallic Materials of Hunan Province College, Hengyang Normal University, Hengyang, Hunan, China

[Ou G.-C.; Yuan L.] Department of Biology and Chemistry, Hunan University of Science and Engineering, Yongzhou, Hunan, China, Key Laboratory of Functional Organometallic Materials of Hunan Province College, Hengyang Normal University, Hengyang, Hunan, China

通讯机构：

[Yuan, X.-Y.] D

Department of Biology and Chemistry, Hunan University of Science and Engineering, Yongzhou, Hunan, China

语种：

英文

关键词：

1,3-Dioxane;2,2′-bis (Hydroxymethyl)butyric acid;4-Chlorobenzaldehyde;Crystal structure;Synthesis

期刊：

Asian Journal of Chemistry

ISSN：

0970-7077

年：

2014

卷：

期：

页码：

6401-6403

DOI：

10.14233/ajchem.2014.16389

机构署名：

本校为其他机构

院系归属：

化学与材料科学学院

摘要：

A new synthetic intermediate 2-(4-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylic acid, derived from the reaction of 2,2′-bis(hydroxymethyl)butyric acid with 4-chlorobenzaldehyde, has been prepared and characterized by IR spectra and 1H NMR spectroscopy. The definitive molecular structure was determined by single-crystal X-ray analyses, which revealed that the title compound belongs to monoclinic system with space group P2(1)/n with a = 12.655(3) A˚, b = 8.260(2) A˚, c = 24.380(6) A˚, β = 92.533(2)°, Mr = 270.70, V = 2545.89(11) A˚3, Dc =...

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Synthesis and crystal structure of 2-(4-chlorophenyl)-5-ethyl-1,3-dioxane-5-carboxylic acid

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