Facile synthesis of Pd/N-doped reduced graphene oxide via a moderate wet-chemical route for non-enzymatic electrochemical detection of estradiol

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成果类型：

期刊论文

作者：

Li, Junhua;Jiang, Jianbo;Zhao, Dan;Xu, Zhifeng;Liu, Mengqin;...

通讯作者：

Xie, Haobin;Qian, Dong

作者机构：

[Liu, Xing; Liu, Mengqin; Deng, Peihong; Xu, Zhifeng; Xie, Haobin; Li, Junhua] Hengyang Normal Univ, Key Lab Funct Met Organ Cpds Hunan Prov, Hengyang 421008, Peoples R China.

[Li, Junhua; Jiang, Jianbo; Zhao, Dan; Qian, Dong] Cent S Univ, Coll Chem & Chem Engn, Hunan Prov Key Lab Chem Power Resources, Hunan Prov Key Lab Efficient & Clean Utilizat Man, Changsha 410083, Hunan, Peoples R China.

[Li, Junhua] Hengyang Normal Univ, Coll Chem & Mat Sci, Hunan Prov Univ Key Lab Funct Organometall Mat, Hengyang 421008, Peoples R China.

[Jiang, Jianbo] Jishou Univ, Coll Chem & Chem Engn, Jishou 416000, Peoples R China.

[Yang, Chunming] Hunan Normal Univ, Coll Chem & Chem Engn, Changsha 410081, Hunan, Peoples R China.

通讯机构：

[Xie, Haobin] H

[Qian, Dong] C

Hengyang Normal Univ, Key Lab Funct Met Organ Cpds Hunan Prov, Hengyang 421008, Peoples R China.

Cent S Univ, Coll Chem & Chem Engn, Hunan Prov Key Lab Chem Power Resources, Hunan Prov Key Lab Efficient & Clean Utilizat Man, Changsha 410083, Hunan, Peoples R China.

语种：

英文

关键词：

Doping (additives);Graphene;High resolution transmission electron microscopy;Nanoparticles;Palladium compounds;Photoelectron spectroscopy;Reduced Graphene Oxide;ELectrochemical detection;Estradiol;N-doped;PD nano particle;Wet-chemical method;Chemical detection

期刊：

Journal of Alloys and Compounds

ISSN：

0925-8388

年：

2018

卷：

769

页码：

566-575

DOI：

10.1016/j.jallcom.2018.08.016

基金类别：

This work was financially supported by National Natural Science Foundation of China (No. 21505035, 21171174, 21472038 and 21603065), Provincial Natural Science Foundation of Hunan (No. 2016JJ3028, 2017JJ2007 and 2016JJ4010), Scientific Research Projects of Education Department of Hunan Province (No. 17K013 and 16A029), Provincial Platform Open Fund Projects of Hengyang Normal University (No. GN16K05 and GD16K02), the Aid Programs for Innovative Team and Key Discipline in Education Department of Hunan Province, and the Hunan Provincial Science and Technology Plan Project (No. 2016TP1007 and 2017TP1001). This work was financially supported by National Natural Science Foundation of China (No. 21505035 , 21171174 , 21472038 and 21603065 ), Provincial Natural Science Foundation of Hunan (No. 2016JJ3028 , 2017JJ2007 and 2016JJ4010 ), Scientific Research Projects of Education Department of Hunan Province (No. 17K013 and 16A029 ), Provincial Platform Open Fund Projects of Hengyang Normal University (No. GN16K05 and GD16K02 ), the Aid Programs for Innovative Team and Key Discipline in Education Department of Hunan Province , and the Hunan Provincial Science and Technology Plan Project (No. 2016TP1007 and 2017TP1001 ).

机构署名：

本校为第一且通讯机构

院系归属：

化学与材料科学学院

摘要：

In this work, Pd-decorated N-doped reduced graphene oxide (Pd/N-RGO) was successfully synthesized by a simple wet-chemical method without using any capping agent and stabilizer. The synthesized Pd/N-RGO composite has been carefully characterized by various techniques. The X-ray photoelectron spectra provide the evidence of successful incorporation of N into the N-RGO sheets, while the presence of Pd nanoparticles with the sizes of 5–20 nm on the N-RGO sheets was confirmed by the transmission electron microscopy. By integrating the advantages o...

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Facile synthesis of Pd/N-doped reduced graphene oxide via a moderate wet-chemical route for non-enzymatic electrochemical detection of estradiol

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