Facile synthesis of Pd/N-doped reduced graphene oxide via a moderate wet-chemical route for non-enzymatic electrochemical detection of estradiol

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成果类型：

期刊论文

作者：

Li, Junhua;Jiang, Jianbo;Zhao, Dan;Xu, Zhifeng;Liu, Mengqin;...

通讯作者：

Xie, Haobin;Qian, Dong

作者机构：

[Liu, Xing; Liu, Mengqin; Deng, Peihong; Xu, Zhifeng; Xie, Haobin; Li, Junhua] Hengyang Normal Univ, Key Lab Funct Met Organ Cpds Hunan Prov, Hengyang 421008, Peoples R China.

[Li, Junhua; Jiang, Jianbo; Zhao, Dan; Qian, Dong] Cent S Univ, Coll Chem & Chem Engn, Hunan Prov Key Lab Chem Power Resources, Hunan Prov Key Lab Efficient & Clean Utilizat Man, Changsha 410083, Hunan, Peoples R China.

[Li, Junhua] Hengyang Normal Univ, Coll Chem & Mat Sci, Hunan Prov Univ Key Lab Funct Organometall Mat, Hengyang 421008, Peoples R China.

[Jiang, Jianbo] Jishou Univ, Coll Chem & Chem Engn, Jishou 416000, Peoples R China.

[Yang, Chunming] Hunan Normal Univ, Coll Chem & Chem Engn, Changsha 410081, Hunan, Peoples R China.

通讯机构：

[Xie, Haobin] H

[Qian, Dong] C

Hengyang Normal Univ, Key Lab Funct Met Organ Cpds Hunan Prov, Hengyang 421008, Peoples R China.

Cent S Univ, Coll Chem & Chem Engn, Hunan Prov Key Lab Chem Power Resources, Hunan Prov Key Lab Efficient & Clean Utilizat Man, Changsha 410083, Hunan, Peoples R China.

语种：

英文

关键词：

N-doped reduced graphene oxide;Pd nanoparticles;Electrochemical detection;Estradiol;Wet-chemical method

期刊：

Journal of Alloys and Compounds

ISSN：

0925-8388

年：

2018

卷：

769

页码：

566-575

DOI：

10.1016/j.jallcom.2018.08.016

基金类别：

National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21505035, 21171174, 21472038, 21603065]; Provincial Natural Science Foundation of HunanNatural Science Foundation of Hunan Province [2016JJ3028, 2017JJ2007, 2016JJ4010]; Scientific Research Projects of Education Department of Hunan Province [17K013, 16A029]; Provincial Platform Open Fund Projects of Hengyang Normal University [GN16K05, GD16K02]; Aid Programs for Innovative Team and Key Discipline in Education Department of Hunan Province; Hunan Provincial Science and Technology Plan Project [2016TP1007, 2017TP1001]

机构署名：

本校为第一且通讯机构

院系归属：

化学与材料科学学院

摘要：

In this work, Pd-decorated N-doped reduced graphene oxide (Pd/N-RGO) was successfully synthesized by a simple wet-chemical method without using any capping agent and stabilizer. The synthesized Pd/N-RGO composite has been carefully characterized by various techniques. The X-ray photoelectron spectra provide the evidence of successful incorporation of N into the N-RGO sheets, while the presence of Pd nanoparticles with the sizes of 5-20 nm on the N-RGO sheets was confirmed by the transmission electron microscopy. By integrating the advantages of the large surface area of N-RGO sheets and good e...

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Facile synthesis of Pd/N-doped reduced graphene oxide via a moderate wet-chemical route for non-enzymatic electrochemical detection of estradiol

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